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Biodegradable foams based on starch, polyvinyl alcohol, chitosan and sugarcane fibers obtained by extrusion BABT
Debiagi,Flávia; Mali,Suzana; Grossmann,Maria Victória Eiras; Yamashita,Fábio.
Biodegradable foams made from cassava starch, polyvinyl alcohol (PVA), sugarcane bagasse fibers and chitosan were obtained by extrusion. The composites were prepared with formulations determined by a constrained ternary mixtures experimental design, using as variables: (X1) starch / PVA (100 - 70%), (X2) chitosan (0 - 2%) and (X3) fibers from sugar cane (0 - 28%). The effects of varying proportions of these three components on foam properties were studied, as well the relationship between their properties and foam microstructure. The addition of starch/PVA in high proportions increased the expansion index and mechanical resistance of studied foams. Fibers addition improved the expansion and mechanical properties of the foams. There was a trend of red and...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Cassava starch; Mechanical properties; Microstructure; Expansion.
Ano: 2011 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132011000500023
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Cascade of Peritectic Reactions in the B-Fe-U System ArchiMer
Dias, M.; Carvalho, P. A.; Dias, A. P.; Bohn, Marcel; Franco, N.; Tougait, O.; Noel, H.; Goncalves, A. P..
The solidification paths for UFeB4, UFe3B2 and UFe4B, ternary compounds, situated along the U:(Fe,B) = 1:5 line in the B-Fe-U phase diagram, are proposed based on x-ray powder diffraction measurements, differential thermal analysis, heating curves and scanning electron microscopy observations complemented with energy and wavelength dispersive x-ray spectroscopies. The compounds melt incongruently and are formed by peritectic reactions. The present work demonstrates the existence of a cascade of peritectic reactions along the U:(Fe,B) = 1:5 composition line, establishes peritectic temperatures and proposes an isopleth diagram along this line.
Tipo: Text Palavras-chave: Microstructure; Phase transformations; Ternary alloy system.
Ano: 2010 URL: http://archimer.ifremer.fr/doc/00002/11369/8168.pdf
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Characteristics of cassava starch fermentation wastewater based on structural degradation of starch granules Ciência Rural
Pereira,Juliane Mascarenhas; Aquino,Ana Carolina Moura de Sena; Oliveira,Daiana Cardoso de; Rocha,Gabriela; Francisco,Alícia de; Barreto,Pedro Luiz Manique; Amante,Edna Regina.
ABSTRACT: Sour cassava starch is a naturally modified starch produced by fermentation and sun drying, achieving the property of expansion upon baking. Sour cassava starch' bakery products can be prepared without the addition of yeast and it is gluten free. The fermentation process associated with this product has been well studied, but the wastewater, with high acidity and richness in other organic compounds derived from starch degradation, requires further investigation. In this study, the structure of solids present in this residue was studied, seeking to future applications for new materials. The solids of the wastewater were spray dried with maltodextrin (MD) with dextrose equivalent (DE) of 5 and 15 and the structure of the powder was evaluated by...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Sour cassava starch; Fermentation; Water; Microstructure.
Ano: 2016 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782016000400732
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Composition and microstructure of magma bodies from effective medium theory ArchiMer
Taylor, Maj; Singh, Sc.
The extent and seismic properties of magma bodies beneath the subsurface are normally ascertained via seismic methods. The seismic properties of such bodies depend on the composition and microstructure of both melt and crystals. Using effective medium theory, we assess the effect of microstructure, geometry and orientation of melt and crystals on the seismic properties, namely P- and S-wave velocities and anisotropy. We find that S-wave velocity and anisotropy are key observables in determining the composition and microstructure of magma bodies.
Tipo: Text Palavras-chave: Composition; Effective medium; Inclusions; Magma bodies; Microstructure; Seismic properties.
Ano: 2002 URL: https://archimer.ifremer.fr/doc/00466/57763/60030.pdf
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Correlation of boron isotopic composition with ultrastructure in the deep- sea coral Lophelia pertusa: Implications for biomineralization and paleo-pH ArchiMer
Blamart, D.; Rollion-bard, C.; Meibom, A.; Cuif, J. -p.; Juillet-leclerc, A.; Dauphin, Y..
Using the CRPG-CNRS Cameca 1270 ion microprobe facility, we have measured boron isotopic compositions (B-11/B-10) in different ultrastructural components of the deep-sea aragonitic scleractinian coral Lophelia pertusa. We observe a systematic difference in B isotopic composition between the Early Mineralization Zone ( EMZ) and adjacent fibrous skeleton. In EMZ the measured delta(11) B values are consistently low. Fibrous aragonite is characterized by systematically higher delta(11) B values but also displays B isotopic heterogeneity associated with specific growth bands in the calyx wall. The magnitude of the observed B isotopic variations cannot be explained by changes in environmental conditions and is likely caused by biological processes involved in...
Tipo: Text Palavras-chave: Boron isotopes; Deep-sea coral; Biomineralization; Aragonite; Microstructure; PH.
Ano: 2007 URL: https://archimer.ifremer.fr/doc/00235/34641/33060.pdf
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Cuticle microstructure as a new tool in systematic paleontology Naturalis
Waugh, David A.; Feldmann, Rodney M..
Fossil decapod cuticle has received little systematic study. The purpose of the present note is to survey the cuticle architecture of eleven extant decapod crabs arrayed within ten families, and to develop a classification scheme of cuticle types suitable for describing fossil and Recent decapod cuticle morphology.
Tipo: Article / Letter to the editor Palavras-chave: Decapoda; Cuticle; Microstructure; Systematic paleontology.
Ano: 2003 URL: http://www.repository.naturalis.nl/record/534333
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Effect of Preheating on Microstructure and Tensile Properties of Friction Stir Welded AA7075 Aluminium Alloy Joints BABT
Poongkundran,R.; Senthilkumar,K..
ABSTRACT The high strength AA7075 aluminum alloy is commonly used in the aerospace components due to its exclusive mechanical properties like lightweight and high strength. This alloy cannot be welded by fusion welding techniques due to solidification cracking which severely degrade the mechanical properties of the joint. In contrast, through friction stir welding (FSW) process solidification relate defects can be eliminated. Anyhow, the strength of friction stir welded joint is influenced by process parameters and tool parameters. These parameters govern the heat input, metal flow, microstructure evolution and mechanical properties of the weld. In normal welding condition, (without preheating) heat is generated by friction force which is produced between...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Aluminum alloy; Preheating; Friction stir welding; Tensile strength; Microstructure.
Ano: 2016 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132016000300404
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Effects of high pressure on texture and microstructure of sea bass (Dicentrarchus labrax L.) fillets ArchiMer
Cheret, Romuald; Chapleau, Nicolas; Delbarre Ladrat, Christine; Verrez-bagnis, Veronique; De Lamballerie, Marie.
High pressure is an innovative non-thermal food-preservation technology. We studied the effect of high-pressure treatment up-to 500 MPa for 5 min on physical characteristics of sea bass fillets after 0, 7, and 14 d of refrigerated storage.. Color results exhibited an increase of lightness and a slight change of hue, which might be imperceptible in cooked fish. High-pressure treatment induced a decrease of exudation and water-holding capacity Pressure treatment above 300 MPa provoked higher fish hardness after storage than in untreated sample, proving the ability of high pressure to improve textural, quality of chilled, stored fish fillet. These assessments were corroborated with microstructure observations. We showed that high-pressure treatment at 500 MPa...
Tipo: Text Palavras-chave: Preservation; Microstructure; Texture profile analysis; High pressure; Fish.
Ano: 2005 URL: http://archimer.ifremer.fr/doc/2005/publication-734.pdf
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Evidence of a Biological Control over Origin, Growth and End of the Calcite Prisms in the Shells of Pinctada margaritifera (Pelecypod, Pterioidea) ArchiMer
Cuif, Jean-pierre; Burghammer, Manfred; Chamard, Virginie; Dauphin, Yannicke; Godard, Pierre; Le Moullac, Gilles; Nehrke, Gernot; Perez-huerta, Alberto.
Consistently classified among the references for calcite simple prisms, the microstructural units that form the outer layer of the Pinctada margaritifera have been investigated through a series of morphological, crystallographical and biochemical characterizations. It is often said that the polygonal transverse shape of the prisms result from the competition for space between adjacent crystals. In contrast to this classical scheme the Pinctada prisms appear to be composed of four successive developmental stages from the concentrically growing disks on the internal side of the periostracum to the morphological, structural and compositional changes in both envelopes and mineral components at the end of the prisms. These latest structural and compositional...
Tipo: Text Palavras-chave: Biomineralization; Bivalve shell; Microstructure; Calcite prisms.
Ano: 2014 URL: http://archimer.ifremer.fr/doc/00249/36039/34574.pdf
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La Biominéralisation de Pecten maximus L. : Anomalies liées aux Perturbations du Milieu ArchiMer
Larvor, Helene.
L'étude du brunissement pathologique des valves de la coquille Saint-Jacques a permis d'identifier différents types d'altérations des mécanismes de la calcification : des détériorations microstructurales concomitantes avec une pigmentation brune anormale de la couche interne des tests. Les mécanismes de biominéralisation contrôlant l'intégration du carbonate de calcium dans les structures coquillières ne sont pas altérés : le taux de calcium, la minéralogie et la composition en acides aminés des matrices organiques cristallines sont équivalents dans les valves brunes et les valves blanches. Par contre, la présence d'une eumélanine, responsable de la coloration brune, est détectée dans les matrices organiques insolubles des régions coquillières aux...
Tipo: Text Palavras-chave: Calcification; Coquille; Mélanine; Microstructure; Pecten maximus; Mollusques; Perturbations environnementales; Biominéralisation.
Ano: 1996 URL: http://archimer.ifremer.fr/doc/00043/15449/12823.pdf
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Milk from different species on physicochemical and microstructural yoghurt properties Ciência Rural
Vianna,Felipe Santana; Canto,Anna Carolina Vilhena da Cruz Silva; Costa-Lima,Bruno; Salim,Ana Paula; Balthazar,Celso Fasura; Costa,Marion Pereira; Panzenhagen,Pedro; Rachid,Rachel; Franco,Robson Maia; Adam Conte-Junior,Carlos; Silva,Adriana Cristina de Oliveira.
ABSTRACT: The aim of the present research was to evaluate differences in chemical properties and physical structure of yoghurt produced with milk from different species (sheep, cow, and goat). For each trial, whole raw sheep (S), cow (C), and goat (G) milk were used to manufacture 4L of yoghurts (Y) from each species (SY, CY, and GY, respectively). The SY demonstrated the greatest (P<0.05) values of total solids, protein, and lipid contents, reflecting on greater (P<0.05) firmness, apparent viscosity and water-holding capacity, and lower (P<0.05) syneresis index than CY and GY. Consequently, SY exhibited a more compact microstructure and homogeneous matrix with fewer pores. Furthermore, CY and GY microstructure contained a greater number of...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Fermented products; Texture; Microstructure; Sheep milk; Goat milk.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782019000600750
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Physicochemical characterization of saccharides powder obtained from yacon roots (Smallanthus sonchifolius) by membrane technology BABT
Alles,Maria Julia Ledur; Tessaro,Isabel Cristina; Noreña,Caciano Pelayo Zapata.
Fructooligosaccharides (FOS) are food ingredients applied due to combination of prebiotic benefits and interesting technological properties, being used as a sugar substitute. The knowledge of their physicochemical characteristics is important for predicting the stability of the food products where they are added. For this reason, a saccharides powder extracted from yacon (Smallanthus sonchifolius) roots by membrane technology and freeze-dried was investigated. Color, water activity (aw), microstructure by Scanning Electron Microscopy coupled to Energy- dispersive X-ray Spectroscopy (SEM-EDS) and crystallinity by X-ray diffraction were evaluated. The obtained product, containing 19.75% FOS, 36.66% glucose and 43.59% fructose (w/w) was a whitish granulated...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Yacon; Fructooligosaccharides; Microstructure; Cristallinity.
Ano: 2013 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132013000600019
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Poly (l-lactide acid) improves complete nano-hydroxyapatite bone scaffolds through the microstructure rearrangement Electron. J. Biotechnol.
Shuai,Cijun; Nie,Yi; Gao,Chengde; Lu,Haibo; Hu,Huanlong; Wen,Xuejun; Peng,Shuping.
Cracks often occur when nano-hydroxyapatite bone scaffolds are fabricated with selective laser sintering, which affect the performance of scaffolds. In this study, a small amount of poly (l-lactide acid) (PLLA) was added into nano-hydroxyapatite (nano-HAP) powder by mechanical blending in order to improve the sintering properties. The nano-HAP powder combined with 1wt % PLLA was sintered under different laser power (5W, 7.5W, 10W, 12.5W, 15W and 20W). The fabricated scaffolds were characterized using Scanning Electron Microscope (SEM), X-ray Diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR) and Micro Hardness Tester. The results showed that nano-HAP particles grew up quickly with the laser power increasing, and there were many strip-like...
Tipo: Journal article Palavras-chave: Hardness; Microstructure; Nano-hydroxyapatite; Thermal properties.
Ano: 2012 URL: http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-34582012000600004
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Preliminary study of age, growth and birthdates of juvenile sardine <Sardina pilchardus> (Walbaum, 1792) and European anchovy Engraulis encrasicolus (Linnaeus, 1758) in the east coast of Tunisia OceanDocs
Khemiri, S.; Gaamour, A..
The microstructures of the otoliths of juvenile sardines (Sardina pilchardus) and anchovies (Engraulis encrasicolus), collected in the East coast of Tunisia, were analyzed in order to estimate age, daily growth and hatch date. The fork length of sardines varied from 48 to 103 mm and estimated age ranged from 105 to 297 days. For the anchovies, the estimated age ranged from 79 to 300 days and the fork length from 42 to 86 mm. The length-age data of both species were fitted to the laird-Gompertz model. The corresponding growth equations were [lt=10.8 exp(2.74(1-exp(-0.006t)))] for sardines and [lt=3.1 exp(3.2(1-exp(-0.02t)))] for anchovies. The instantaneous growth rates of the juvenile of both species in the East of Tunisia were in agreement with the data...
Tipo: Journal Contribution Palavras-chave: Age determination; Daily; Growth; Hatching; Microstructure; Otoliths; Population structure; Age determination; Growth; Otoliths; Population structure; Hatching; Http://aims.fao.org/aos/agrovoc/c_24110; Http://aims.fao.org/aos/agrovoc/c_3394; Http://aims.fao.org/aos/agrovoc/c_27091; Http://aims.fao.org/aos/agrovoc/c_6115; Http://aims.fao.org/aos/agrovoc/c_3504.
Ano: 2005 URL: http://hdl.handle.net/1834/3797
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Preparation techniques alter the mineral and organic fractions of fish otoliths: insights using Raman micro-spectrometry ArchiMer
Jolivet, Aurelie; Fablet, Ronan; Bardeau, Jean-francois; De Pontual, Helene.
The high spatial resolution analysis of the mineral and organic composition of otoliths using Raman micro-spectrometry involves rigorous protocols for sample preparation previously established for microchemistry and trace elements analyses. These protocols often include otolith embedding in chemically neutral resin (i.e., resins which do not contain, in detectable concentration, elements usually sought in the otoliths). Such embedding may however induce organic contamination. In this paper, Raman micro-spectrometry reveals the presence of organic contamination onto the surface obtained from the use of epoxy resin, specifically Araldite. This contamination level varies depending on otolith structures. Core and checks, known as structural discontinuities,...
Tipo: Text Palavras-chave: Epoxy resin; Otolith composition; Microstructure; Raman spectrometry.
Ano: 2013 URL: http://archimer.ifremer.fr/doc/00138/24965/26372.pdf
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Properties of extruded xanthan-starch-clay nanocomposite films BABT
Melo,Cristina de; Garcia,Patrícia Salomão; Grossmann,Maria Victória Eiras; Yamashita,Fábio; Dall'Antônia,Luiz Henrique; Mali,Suzana.
The aim of this work was to manufacture the biodegradable nanocomposite films by extrusion from different combinations of cassava starch, xanthan gum and nanoclays (sodium montmorillonite - MMT- Na) and to characterize them according to their microstructure, optical, mechanical and barrier properties. Films were manufactured from nine starch/xanthan/nanoclay combinations, containing glycerol as plasticizer. Scanning electron microscopy (SEM) of the starch-xanthan extruded films showed reticulated surface and smooth interior, indicating that the gum was mostly concentrated on the surface of the films, while starch/xanthan/nanoclays films showed a more homogeneous surface, suggesting that the introduction of nanoclays provided a better biopolymeric...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Film blowing; Cassava starch; Microstructure; Mechanical properties; Water vapor permeability.
Ano: 2011 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132011000600019
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Shell repair process in the green ormer Haliotis tuberculata: A histological and microstructural study ArchiMer
Fleury, C; Marin, F; Marie, B; Luquet, G; Thomas, J; Josse, C; Serpentini, A; Lebel, J.
In the present paper, juvenile and adult shells of the green ormer Haliotis tuberculata ('Oreille de Saint-Pierre') were perforated in a zone close to the shell edge and the shell repair process was followed at two levels: (1) by observing the histology of the calcifying mantle in the repair zone and (2) by analyzing with SEM the microstructure of the shell repair zone. Histological data clearly show the presence of calcium carbonate granules into the connective tissues, but not in the epithelial cells. This suggests that calcium carbonate granules are synthesized by sub-epithelial cells and actively transported through the epithelium to the repair zone, via a process which may be similar to that described by Mount et al. [Mount, A.S., Wheeler, A.P.,...
Tipo: Text Palavras-chave: Microstructure; Mantle epithelium; Biomineralization; Calcium carbonate; Shell repair; Gastropod.
Ano: 2008 URL: https://archimer.ifremer.fr/doc/2008/publication-4377.pdf
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Stability and microstructure of powdered pulp of the Palmer mango obtained by the process of lyophilisation Rev. Ciênc. Agron.
Costa,Laiana Oliveira; Lara Junior,Jovan Marques; Costa,José Maria Correia da; Afonso,Marcos Rodrigues Amorim; Rodrigues,Sueli; Wurlitzer,Nédio Jair.
ABSTRACT The aim of this work was to study the stability of powdered mango pulp obtained through the process of lyophilisation, as well as its structural characteristics using electron microscopy analysis. In response to an earlier experimental design using maltodextrin concentrations of 0%, 10%, 20% and 30% and periods of 24 and 30 hours, the condition of 20% maltodextrin and 24 hours drying was chosen as the best for drying mango in a freeze dryer. The stability study was therefore carried out using powdered mango pulp obtained under the above best-drying conditions, stored for 90 days and monitored every two weeks by analysis of the moisture, ascorbic acid content, b* colorimetric parameter and hygroscopicity. Storage was at room temperature (27 °C) in...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Drying; Maltodextrin; Hygroscopicity; Microstructure.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1806-66902019000200251
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Tensile strength, friability and organic carbon in an oxisol under a crop-livestock system Scientia Agricola
Guimarães,Rachel Muylaert Locks; Tormena,Cássio Antonio; Alves,Sérgio José; Fidalski,Jonez; Blainski,Éverton.
The crop-livestock system can promote soil compaction in surface layers, mainly due to animal trampling. However, plants and their root growth, in interaction with animal trampling, can decrease the deleterious changes in soil structure caused by this system. Up to the present time, the physical soil modifications in crop-livestock systems, including oat and ryegrass crops for winter animal forages are unknown. The objective of this study was to quantify and to relate tensile strength, friability and soil organic carbon in an Oxisol under a crop-livestock system. The study was conducted in Campo Mourão - Paraná, Brazil. Four forage heights were used for the winter forages: 7, 14, 21 and 28 cm. For each forage height, five soil blocks were randomly...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Aggregate; Soil structure; No-tillage; Soil physical quality; Microstructure.
Ano: 2009 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-90162009000400011
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Uterine Gland Microstructure in the Pregnant and the Non-pregnant Lesser Galago (Galago senegalensis) International Journal of Morphology
Njogu,Allan; Owiti,George Otiang'a; Oduor-Okelo,Dominic.
The histology and the ultrastructure of the uterine glands of the lesser bushbaby (Galago senegalensis) were studied in six specimens (5 pregnant and one non pregnant) which were fixed partly with bouin's fixative and part with 2.5% glutaraldehyde in 0.1 M cacodylate buffer. An overview of the main results revealed uterine glands in the non-pregnant uterus are rudimentary and scarce within the mucosa. In early pregnancy (first trimester) the uterine glands profiles appear in clusters. In late stage pregnancy (third trimester) the uterine gland profiles appear opposite chorionic vesicles. In the later stages of gestation maternal glandular epithelium consisted mainly of simple columnar epithelium. The cells had abundant flattened cisternae of granular...
Tipo: Journal article Palavras-chave: Lesser bushbaby; Uterine gland; Microstructure.
Ano: 2013 URL: http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-95022013000200067
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